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Homogenizing-Dispersing
A dispersion is simply the transport of one phase
or ingredient (liquid, solid, gas) into a main continuous
phase (typically liquid), with which it would normally
be immiscible. The fluid is said to be homogenized
when sufficient energy input results in a final product
that resembles a mono-dispersion fluid, with no differentiation
between separate components. The system is considered
colloidal when one or more of the components has at
least one dimension that is less than a micrometer
(10-6 m). In liquid mixing, we can classify the various
systems as Suspensions (Solid/Liquid), Emulsions (Liquid/Liquid)
and Foams (Gas/Liquid).
High
shear mixers create an intense, concentrated energy
input that can produce a superior dispersion in significantly
less time than traditional mixing methods. Below are
a few common applications that IKA® mixers are used to produce:
Cosmetic
Applications
Creams, Ointments, and Lotions
Creams, ointments, and lotions include a wide variety
of products, which are manufactured in a similar manner.
The process generally involves dispersion and hydration
of thickening agents, colors, perfumes, and active
ingredients into either an oil or water phase. The
two phases are then emulsified, cooled, and packaged.
The challenges to the manufacturer are to effectively
hydrate all the powders (which are often difficult
to disperse), emulsify the phases, and maintain a
consistent product. Using IKA® Works Mixers addresses all of these concerns.
Products
that are moderately difficult to homogenize can be
produced with the Shear Pump SP, or Hi-Energy Disperser
HED for continuous or semi-continuous processes, and
with the Rototron RT or Turbotron RK/RF for batch
processes. Difficult to homogenize products can be
produced with the Ultra Turrax UTL or Dispax Reactor
DR for continuous or semi-continuous processes, and
with the Ultra Turrax for batch processes.
Suspending
-Wet Milling (Solid-Liquid)
Suspending is dispersing of solid particles in a liquid.
It is often desirable to reduce the particle size
of the solids in conjunction with dispersing, and
this is often referred to as wet milling. With the
use of high shear mixers and sufficient energy input,
the final product will become homogenized. Below is
a list of some typical applications, and which IKA® mixer provides the best solution:
Suspensions
are easily accomplished with a Hi-Energy Disperser
HED or Shear Pump SP for in-line processes, and the
Ultra Turrax for batch or in-line processes. Wet milling
requires more energy than suspending, and can vary
widely, depending on the product. In order of increasing
milling energy, IKA® offers the Ultra Turrax UTL, Dispax Reactor DR, Super
Dispax Reactor™ DRS, Colloid Mill MK and the
Cone Mill MKO. Batch processing can be accomplished
with the Ultra Turrax™.
Emulsifying
(Liquid-Liquid Systems)
Emulsifying is the process of dispersing one liquid
in a second immiscible liquid, such as oil dispersed
in water. A colloidal suspension is a system comprising
particles dispersed in a liquid that do not settle
out of solution due to their extremely small size
of less than one micrometer. In order to achieve the
stable emulsion, a suitable amount of energy input
is required to produce the droplet size that is necessary.
A few examples of some common emulsions are:
Many
emulsions are easily accomplished using moderate energy,
and therefore, the Hi-Energy Disperser HED or Shear
Pump SP is satisfactory for in-line processes, and
the Rototron RT for batch processes. When the droplet
size required is less then 10 microns, or sub-micron,
higher energy input is required. In order to produce
these smaller droplet sizes, or when the concentrations
are high, IKA® offers the following mixers Ultra Turrax™ UTL,
Dispax Reactor DR, Super Dispax Reactor DRS and Colloid
Mill MK. Batch processing can be accomplished with
the Ultra Turrax.
Dissolving –Molecular/Colloidal
Below is a list of some typical dissolving applications,
and which IKA® mixer provides the best solution:
Most
dissolving applications are easily accomplished with
a Hi-Energy Disperser HED or Shear Pump SP for in-line
processes, and the Ultra Turrax for batch or in-line
processes. Difficult to dissolve materials may require
a mixer with higher energy input. In addition, to
reduce or eliminate re-circulating, one of the following
IKA® mixers may be required, in order of increasing energy,
IKA® offers the Ultra Turrax UTL, Dispax Reactor™
DR, Super Dispax Reactor DRS, Colloid Mill MK. Batch
processing can be accomplished with the Ultra Turrax.
Powder-Liquid
Incorporation
Incorporating powders into liquids offers many challenges
to processors. The powders may be difficult to wet
out, and may produce fish-eyes if not effectively
dispersed into the liquid. The powders are often added
to a vessel by dumping bags into the top, creating
a plume of dust and creating a possible health hazard.
Eductors, blenders, and other powder addition equipment
will often clog, or not perform as well as desired,
or the system is too complex to clean and maintain.
IKA® has developed unique, new technology that obsoletes
many of these older technologies. IKA® offers a complete line of powder-liquid mixers that
offers more solutions than any other mixer manufacturer.
Below is a list of some typical applications, and
which IKA® mixer provides the best solution:
Cosmetic Applications
- Carbopol®
Carbopol® (Carbopol® is a registered trademark of Noveon, Inc) is one of
the most commonly used carbomers, a family of ingredients
used in cosmetics to thicken, suspend, stabilize,
and emulsify a wide range of recipes. Carbopol® is a light, dusting powder, which will easily raft
(float) on a liquid surface unless substantial agitation
is applied. Once incorporated into the liquid, the
powder often forms agglomerates or fish-eyes. The
final viscosity is also sensitive to pH. Therefore,
a base (high pH material) must often be added to achieve
the finished viscosity. IKA® Works range of high shear mixers offer cosmetics manufacturers
solutions to all the above concerns.
ADVANTAGES OF IKA® WORKS MIXERS FOR THE HYDRATION OF CARBOPOL®
- Easy
incorporation into liquid. IKA® offers multiple mixer designs, both batch and inline,
suitable for dispersing Carbopol® . The CMS and MHD mixers allow the powder to be
added directly to the liquid stream, without dusting
or aeration.
- Smooth
consistent product. The high shear rotor / stator
action of an IKA® Works Mixer ensures no agglomerates are present
in the final product.
- Decreased
operator input. IKA® Mixers are not as sensitive to rates of ingredient
addition as other devices. IKA® Works also offers their customers the option of
complete systems with automated powder feed and
PLC controls.
- Decreased
raw materials costs. The absence of agglomerates
allows processors to avoid filtration and wasted
powder. Also, the intimate dispersion achieved with
an IKA® Works rotor / stator mixer ensures full hydration
of powders and rapid pH adjustment with tight control,
avoiding excessive caustic usage.
IKA® MIXERS SUITABLE FOR HYDRATING CARBOPOL®
- Batch: RT, RKG, MSM, UTC, UTE,
UTS
- Inline: HED, UTL, DR, DRS, CMS,
MHD
Xanthan
Gum
Pigments
Pectin
Clays
When
adding solids in a batch process, the Rototron RT
will quickly incorporate and disperse the solids in
the vessel, for higher dispersing energy, the Ultra
Turrax is recommended. To process in a re-circulating
configuration, the CMS will rapidly wet out and disperse
the solids. The CMS can also be used in a continuous
system, and will handle large volumes of solids. IKA’s
patented MHD is the best choice for continuous processes
when aeration must be reduced to a minimum, accurate
feed rates are required, or when the viscosity of
the liquid is high. The MHD also has the widest variety
of mixing tools available, and can provide enough
energy to disperse even the most difficult products
in one pass. The MHD is the only powder-liquid mixer
in the industry that does not require vacuum to incorporate
the solids, thus, eliminating the aeration that is
inherent in other designs.
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